Industrial Consultancy & Sponsored Research (IC&SR) , IIT Madras

A Continuous Automated System and Method for Sensing of Nitrite in Water

Categories for this Invention

Technology: Water quality monitoring

Category: Environmental Engineering Chemistry & Chemical Analysis

Industry: Water & Wastewater Management

ApplicationBoth domestic and industrial applications for real-time online water quality monitoring of Nitrite.

Market: The global market size  of water Quality Monitoring Market is likely to grow with a CAGR of 5.51% during the forecast period 2023-2030, and reach a revenue of $8275.72 million by 2030, from $5420.38 million in 2022.

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Problem Statement

  • Water quality is crucial for all living organisms, but anthropogenic sources like livestock waste, organic waste, and fertilizers cause significant contamination.
  • Early detection of nitrite and nitrate in water is essential to prevent further damage and prevent environmental issues.
  • Conventional methods for detecting contaminants include spectrophotometric, chemiluminescence, electrochemical, chromatography, capillary electrophoresis, and spectrofluorimetric.
  • However, these methods require expert assistance and are sensitive but expensive.
  • Automated real-time monitoring systems are needed to address challenges and improve water quality, including low-cost sensors and environmentally friendly systems.

Technology

  • A real-time continuous monitoring automated system  for sensing of nitrite in water by colorimetric method, the system comprising:
  • Detection Chamber  configured to do a preliminary colour analysis of a sample and cuvette to hold the sample and wherein the sample is pumped to the chamber.
  • Driver Circuit  configured to enable pumping of the sample and a reagent to the detection chamber.
  • An automated mixing mechanism with a servo motor to mix sample with reagent and a light source for incubation.
  • Photo detector for record the absorbance of light by the sample and the sample reagent mix to obtain a secondary color analysis.
  • A Microcontroller and Relay module for automated operation, and
  • A Rinse and Drain Mechanism for cleaning the cuvette for fresh sample sensing.
  • The system uses white light with good sensitivity in green and blue ranges, focusing on a 20mm cuvette with a 7ml volume capacity.
  • A Plano-convex lens focuses light onto a color sensor in a photo detector, recording absorbance at 543 nm. Nitrite concentration is detected using a reagent.
  • The system minimizes interference from external disturbances and uses ratio metric analysis to remove stain and color effects.

Key Features / Value Proposition

  • The system utilizes online sensing techniques to monitor water quality in aqueous systems in real-time, utilizing a fully automated and portable system.
  • The online colorimetric sensing technique is a method that is independent of the stain’s effects on the detection chamber and the color of the tested sample.
  • The study aims to provide fast, accurate, and continuous measurements of nitrite in water.
  • The detection process is automated and results are verified using cuvette staining and external-colored compounds in the water system.
  • The online nitrite detection system is reliable and automated, detecting nitrite in the 0-10 mg/L range.
  • It eliminates stain or color development, and no humidity limitations are present.
  • Low-cost, portable, and automated devices, with a readily available test kit.

Questions about this Technology?

Contact For Licensing

sm-marketing@imail.iitm.ac.in
ipoffice2@iitm.ac.in

Research Lab

Prof. Boby George

Department of Electrical Engineering

Prof. Ligy Philip

Department of Civil Engineering

Intellectual Property

  • IITM IDF Ref. 2588
  • Patent No: IN 533197

Technology Readiness Level

TRL-4

Experimentally validated in Lab

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