Industrial Consultancy & Sponsored Research (IC&SR) , IIT Madras

Method for Generating White Light using WL- GQD

Categories for this Invention

Technology: Generating white light by Graphene quantum dots  (WL-GQD)

Category: Quantum Technology & Bioimaging

Industry: Optical and Biotechnology  Industry.

Application: Material science, Device fabrication, sensing, and Bio-imaging.

Market: The global market size valued at USD 160 million in 2022 and is anticipated to reach a value of USD 203.9 million by 2030 expanding at a CAGR of 3.2%

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Problem Statement

  • Quantum dots are quantum materials with electrons confined in three dimensions (3D).
  • They are used in light emitting applications, sensing, and medicine.
  • Carbon-based quantum dots (CQD) are cost-effective and have fluorescence properties ranging from UV to NIR.
  • Fluorescence quantum yield is crucial in applications like LEDs, bio imaging, and turn-off sensors.
  • Fluorescence quantum yield can be improved by doping with components like nitrogen and sulfur.
  • Fluorescence emission wavelength can be regulated by changing nano particle size and optical excitation to obtain different colors.
  • Conventional methods use harmful acids as precursors, making the fabrication process bio-in_compatible
  • There is a need for generating broad white light emission from a single species with  biocompatible   cost effective percursurs.

Technology

  • Mixing a Polycyclic Aromatic Hydrocarbon as a Carbon Precursor and
  • A Heteroatoms Co-doping Compound in Deionized (Di) Water to Obtain a Mixture, Wherein the Polycyclic aromatic hydrocarbon Is Naphthalene and the Heteroatoms Co-doping Compound is thiourea;
  • Fabricating the Heteroatoms Co-doped Graphene Quantum Dots by
  • Performing a Thermal Procedure on the Mixture;
  • Obtaining the WL-GQD by drying residue of the fabricated Heteroatoms Co-doped Graphene Quantum Dots and
  • Generating the White Light By Using the obtained WL-GQD

Key Features / Value Proposition

Thermal procedure:

  • Performed in an autoclave at 180℃ for 8 hours.

Fabrication:

  • Stirring 1 gm of naphthalene in 80 ml of concentrated nitric acid for 12 hours.
  • Nitration of naphthalene is used to fabricate heteroatoms co-doped graphene quantum dots.
  • The dried residue is obtained using solvent acetone and dried to obtain the WL-GQD.

White light formation:

  • Generated by dispersing the WL-GQD in dimethylformamide (dmf) and polyvinyl alcohol (pva).
  • The heteroatoms co-doping compound includes nitrogen and sulfur doping.

Centrifugation:

  • The fabricated heteroatoms co-doped graphene quantum dots are centrifuged at 12000 rpm for 30 minutes.
  • Sediment from the centrifuged heteroatoms co-doped graphene quantum dots is filtered and dialyzed for 2 days.

Obtaining NS-GQD:

  • The filtered heteroatoms co-doped graphene quantum dots are freeze-dried for a day to obtain NS-GQD

Advantages

  • Utilizes environmentally friendly components like polycyclic aromatic hydrocarbon and heteroatoms co-doping compound.
  • Wl-gqd is a single carbon quantum dots (CQD), making mass production easy and cost-effective.

Questions about this Technology?

Contact For Licensing

sm-marketing@imail.iitm.ac.in
ipoffice2@iitm.ac.in

Research Lab

Prof. Prem B. Bisht

Ultrafast lasers and optical amplifiers

Department of  Physics

Intellectual Property

  • IITM IDF Ref. 2228
  • Patent No: IN 544251

Technology Readiness Level

TRL- 3

Experimental Proof of Concept

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